5F8C
Rv2258c-unbound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
| Synchrotron site | PAL/PLS |
| Beamline | 7A (6B, 6C1) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-04-03 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.92019 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 109.254, 140.635, 97.239 |
| Unit cell angles | 90.00, 98.56, 90.00 |
Refinement procedure
| Resolution | 27.250 - 1.830 |
| R-factor | 0.19252 |
| Rwork | 0.191 |
| R-free | 0.22599 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.269 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.8.0124) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.250 | 1.860 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Number of reflections | 127941 | |
| <I/σ(I)> | 28.7 | 2.9 |
| Completeness [%] | 99.9 | |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 296 | sodium malonate, PEG 3350 |
