5F8B
Crystallographic Structure of PsoE with Co
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-20 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 123.331, 123.331, 75.638 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.626 - 2.540 |
R-factor | 0.1969 |
Rwork | 0.191 |
R-free | 0.24670 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.823 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.540 |
Number of reflections | 21207 |
<I/σ(I)> | 21.38 |
Completeness [%] | 99.8 |
Redundancy | 11.57 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEGmme 5000 |