5F6A
Drosophila Melanogaster Cycle W398A PAS-B with Empty Pocket
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-05 |
Detector | DECTRIS PILATUS3 R 100K-A |
Wavelength(s) | .987 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.999, 44.523, 38.185 |
Unit cell angles | 90.00, 115.32, 90.00 |
Refinement procedure
Resolution | 34.516 - 1.930 |
R-factor | 0.2257 |
Rwork | 0.223 |
R-free | 0.25040 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.645 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.960 |
High resolution limit [Å] | 1.930 | 5.240 | 1.930 |
Rmerge | 0.097 | 0.058 | 0.486 |
Rmeas | 0.117 | 0.070 | 0.629 |
Rpim | 0.064 | 0.038 | 0.395 |
Total number of observations | 19318 | ||
Number of reflections | 6663 | ||
<I/σ(I)> | 4.3 | ||
Completeness [%] | 78.5 | 100 | 34.7 |
Redundancy | 2.9 | 3.2 | 1.6 |
CC(1/2) | 0.987 | 0.596 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | Ammonium Sulfate |