5F4L

HIV-1 gp120 complex with JP-III-048

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BSRF BEAMLINE 1W2B
Synchrotron site	BSRF
Beamline	1W2B
Temperature [K]	170
Detector technology	CCD
Collection date	2014-04-02
Detector	APEX II CCD
Wavelength(s)	0.9791
Spacegroup name	C 2 2 21
Unit cell lengths	67.159, 127.806, 192.470
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.439 - 2.700
R-factor	0.2503
Rwork	0.248
R-free	0.28810
RMSD bond length	0.004
RMSD bond angle	0.811
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.8.4_1496)

Data quality characteristics

	Overall
Low resolution limit [Å]	45.276
High resolution limit [Å]	2.700
Rmerge	0.119
Number of reflections	23229
<I/σ(I)>	12.5
Completeness [%]	99.9
Redundancy	10.88

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		290	PEG 1500, magnesium chloride, imidazole