5EZT

Peracetylated Bovine Carbonic Anhydrase II

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	OTHER
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2007-07-12
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	P 2 21 21
Unit cell lengths	45.701, 63.309, 93.211
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	23.810 - 1.540
R-factor	0.21067
Rwork	0.209
R-free	0.23888
RMSD bond length	0.013
RMSD bond angle	1.526
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	23.810
High resolution limit [Å]	1.540
Number of reflections	34193
<I/σ(I)>	26.7
Completeness [%]	100.0
Redundancy	1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	277.15	1.6M ammonium sulfate, tris