5EZO
Crystal Structure of PfCyRPA in complex with an invasion-inhibitory antibody Fab.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-14 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.000000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 95.801, 44.681, 121.336 |
Unit cell angles | 90.00, 108.03, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 43.000 | 3.720 | |
High resolution limit [Å] | 3.630 | 16.230 | 3.630 |
Rmerge | 0.497 | 0.044 | 2.673 |
Rmeas | 0.595 | 0.054 | 3.181 |
Total number of observations | 37178 | ||
Number of reflections | 11401 | 143 | 855 |
<I/σ(I)> | 2.63 | 14.35 | 0.4 |
Completeness [%] | 99.1 | 92.9 | 98.7 |
Redundancy | 3.3 | 3.3 | |
CC(1/2) | 0.921 | 0.998 | 0.350 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | 0.1 M sodium citrate pH 5.5, 17 % PEG 5000 MME, 0.2 M NDSB-201 |