5EZI
Crystal Structure of Fab of parasite invasion inhibitory antibody c1 - hexagonal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 1970-01-31 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 82.700, 82.700, 361.880 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.154 - 1.610 |
R-factor | 0.1961 |
Rwork | 0.195 |
R-free | 0.22090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | homology model |
RMSD bond length | 0.006 |
RMSD bond angle | 0.887 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.900 | 1.670 |
High resolution limit [Å] | 1.610 | 1.610 |
Number of reflections | 96028 | |
<I/σ(I)> | 8.54 | 0.84 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.8 | 16.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 1.6 M sodium citrate pH 6.5 |