5EY5
LBCATS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-05-14 |
| Detector | DECTRIS PILATUS 200K |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 95.963, 162.996, 78.058 |
| Unit cell angles | 90.00, 93.78, 90.00 |
Refinement procedure
| Resolution | 47.255 - 1.972 |
| R-factor | 0.1811 |
| Rwork | 0.178 |
| R-free | 0.23200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2j9x |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.851 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.250 | 2.043 |
| High resolution limit [Å] | 1.972 | 1.972 |
| Rmerge | 0.082 | 0.459 |
| Number of reflections | 81220 | |
| <I/σ(I)> | 8.7 | 1.93 |
| Completeness [%] | 97.0 | 81 |
| Redundancy | 3.7 | 2.6 |
| CC(1/2) | 0.996 | 0.801 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | sodium citrate tribasic dehydrate, PEG 6000 |
