5EXU
Reversibly photoswitching protein Dathail, Ensemble refinement
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-10-17 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.542 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 76.250, 81.180, 39.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.180 - 1.650 |
R-factor | 0.1711 |
Rwork | 0.168 |
R-free | 0.20990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.016 |
RMSD bond angle | 1.705 |
Data reduction software | iMOSFLM |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.180 | 1.702 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.063 | 0.304 |
Number of reflections | 29829 | |
<I/σ(I)> | 10.91 | 2.18 |
Completeness [%] | 98.6 | 88.1 |
Redundancy | 5.1 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Magnesium Chloride, 0.1M Bis-Tris:HCl pH 6.5, 25% PEG 3350 |