5EWU
Crystal structure of the Arabidopsis thaliana C-terminal Chlh at 1.25A
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-06-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.099, 72.776, 72.911 |
Unit cell angles | 90.00, 109.76, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.250 |
R-factor | 0.16971 |
Rwork | 0.169 |
R-free | 0.18404 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.154 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHARP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.250 |
Number of reflections | 168362 |
<I/σ(I)> | 45 |
Completeness [%] | 89.8 |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | PEG, NaCl |