5ET2
Lambda-Ru(TAP)2(dppz)]2+ bound to d(TTGGCGCCAA)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-16 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 42.380, 42.380, 39.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.830 - 1.390 |
R-factor | 0.16708 |
Rwork | 0.166 |
R-free | 0.18519 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 2.103 |
Data reduction software | xia2 |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.830 | 1.430 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.071 | |
Number of reflections | 7598 | |
<I/σ(I)> | 11.9 | 2.2 |
Completeness [%] | 99.4 | 99.8 |
Redundancy | 5.9 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 292 | 1uL 2mM single stranded DNA, 1uL 4mM rac-RuTAP2dppz, 6ul of a solution containing 40mM Na-cacodylate pH 7, 12mM spermine, 20mM BaCl2, 80mM KCl, 10% 2-methyl-2,4-pentanediol. |