5EST
Crystallographic analysis of the inhibition of porcine pancreatic elastase by a peptidyl boronic acid: structure of a reaction intermediate
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.280, 57.560, 75.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.200 * |
Rwork | 0.150 |
RMSD bond length | 0.017 |
RMSD bond angle | 2.400 |
Refinement software | EREF |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.039 * |
Total number of observations | 10569 * |
Number of reflections | 11021 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PPE solution | 1.4 (%(w/v)) | |
2 | 1 | reservoir | sodium phosphate | 0.1 (M) | |
3 | 1 | reservoir | sodium sulfate | 0.1 (M) |