5ERS
GephE in complex with Mg(2+) - AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-23 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9640 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 87.002, 99.278, 112.791 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.639 - 1.700 |
R-factor | 0.1547 |
Rwork | 0.153 |
R-free | 0.17850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pd0 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.370 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.640 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.133 | 1.081 |
Number of reflections | 53903 | |
<I/σ(I)> | 9.2 | 1.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.5 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 0.1 M sodium acetate, 34% MPD |