5ERR
GephE in complex with Mg(2+) - ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-23 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9640 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 87.681, 99.534, 113.029 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.841 - 1.650 |
R-factor | 0.158 |
Rwork | 0.157 |
R-free | 0.18340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pd0 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.149 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.841 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.091 | 0.998 |
Number of reflections | 59012 | |
<I/σ(I)> | 12.3 | 1.7 |
Completeness [%] | 99.0 | 98.1 |
Redundancy | 6.8 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 0.1 M sodium acetate, 20 % MPD |