5EP0
Quorum-Sensing Signal Integrator LuxO - Receiver+Catalytic Domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9782 |
Spacegroup name | P 61 |
Unit cell lengths | 116.149, 116.149, 71.174 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.091 - 1.600 |
R-factor | 0.1718 |
Rwork | 0.171 |
R-free | 0.19590 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.053 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.10-2155_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 35.000 | 35.000 | 1.630 |
High resolution limit [Å] | 1.600 | 4.340 | 1.600 |
Rmerge | 0.048 | 0.026 | 0.651 |
Rmeas | 0.052 | 0.028 | 0.700 |
Rpim | 0.018 | 0.010 | 0.257 |
Total number of observations | 563802 | ||
Number of reflections | 72082 | ||
<I/σ(I)> | 8.2 | ||
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 7.8 | 7.9 | 7.3 |
CC(1/2) | 0.999 | 0.883 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 100 mM sodium buffer pH5.5, 2 M ammonium sulfate |