5EFX
Crystal structure of Rho GTPase regulator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 37.948, 81.825, 119.830 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.177 - 2.451 |
R-factor | 0.2188 |
Rwork | 0.217 |
R-free | 0.25300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4d0n |
RMSD bond length | 0.009 |
RMSD bond angle | 1.213 |
Data reduction software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.510 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.068 | 0.361 |
Number of reflections | 7006 | |
<I/σ(I)> | 60.5 | 8.29 |
Completeness [%] | 97.2 | 77.2 |
Redundancy | 12.5 | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 289.15 | 0.2M Sodium Nitrate, 20% PEG 3350, PH 6.8 |