5EE3
COMPLEX STRUCTURE OF OSYCHF1 WITH AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 160 |
Detector technology | CCD |
Collection date | 2014-05-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.086, 112.390, 115.023 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.900 |
R-factor | 0.22897 |
Rwork | 0.227 |
R-free | 0.26076 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.163 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | BALBES |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.900 |
Number of reflections | 20818 |
<I/σ(I)> | 19.2 |
Completeness [%] | 99.9 |
Redundancy | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG |