5EDL
Crystal structure of an S-component of ECF transporter
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-06-15 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.978 |
| Spacegroup name | I 4 2 2 |
| Unit cell lengths | 70.713, 70.713, 196.839 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.579 - 1.950 |
| R-factor | 0.1965 |
| Rwork | 0.195 |
| R-free | 0.21750 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.916 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | SHELXDE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.210 | 2.000 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.103 | 0.791 |
| Number of reflections | 18753 | |
| <I/σ(I)> | 11.2 | 2.2 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 7 | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 291 | PEG1000, disodium hydrogen phosphate, citric acid, lithium sulfate |
