5ECO
Crystal Structure of FIN219-FIP1 complex with JA, Leu and Mg
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-08 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.9762-0.97622 |
Spacegroup name | P 1 |
Unit cell lengths | 53.759, 53.836, 192.574 |
Unit cell angles | 90.07, 89.96, 113.53 |
Refinement procedure
Resolution | 23.483 - 1.800 |
R-factor | 0.2236 |
Rwork | 0.222 |
R-free | 0.23880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4epl |
RMSD bond length | 0.009 |
RMSD bond angle | 1.780 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 3.880 | 1.800 |
Rmerge | 0.066 | 0.045 | 0.443 |
Total number of observations | 316315 | ||
Number of reflections | 174895 | ||
<I/σ(I)> | 6.9 | ||
Completeness [%] | 94.9 | 93.2 | 95.9 |
Redundancy | 1.8 | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 297 | 0.2 M sodium acetate trihydrate, 0.1 M Tris-HCl, 30%(w/v) PEG 3000 |