5E6P
PlexinB2 cytoplasmic region/PDZ-RhoGEF PDZ domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-02-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | .979237 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 126.152, 126.152, 211.465 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.530 - 3.215 |
R-factor | 0.2562 |
Rwork | 0.254 |
R-free | 0.29660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ig3 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.754 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.260 |
High resolution limit [Å] | 3.200 | 3.200 |
Number of reflections | 16847 | |
<I/σ(I)> | 56 | 1.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 30.1 | 27.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 293 | 0.2 M K/Na tartrate, 0.1 M Na citrate pH 5.3, 1.4 M ammonium sulfate |