5DUP
Influenza A virus H5 hemagglutinin globular head in complex with antibody AVFluIgG03
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-06-30 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | P 6 |
| Unit cell lengths | 132.664, 132.664, 87.957 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.938 - 3.052 |
| R-factor | 0.2073 |
| Rwork | 0.199 |
| R-free | 0.25700 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.352 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.940 |
| High resolution limit [Å] | 3.050 |
| Number of reflections | 16857 |
| <I/σ(I)> | 12.1 |
| Completeness [%] | 100.0 |
| Redundancy | 7.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2M Potassium sodium tartrate tetrahydrate, 20% w/v Polyethylene glycol 3350 |
