5DU7
Crystal structure of ldtMt2 at 1.79 Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 61.644, 75.534, 94.143 |
Unit cell angles | 89.04, 89.96, 92.76 |
Refinement procedure
Resolution | 50.000 - 1.790 |
R-factor | 0.1716 |
Rwork | 0.170 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vyn |
RMSD bond length | 0.020 |
RMSD bond angle | 1.991 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.610 | 1.700 |
Rmerge | 0.068 | 0.042 | 0.800 |
Rmeas | 0.078 | 0.049 | |
Rpim | 0.041 | 0.025 | 0.544 |
Total number of observations | 676223 | ||
Number of reflections | 153919 | ||
<I/σ(I)> | 7.6 | ||
Completeness [%] | 97.3 | 98.3 | 95.7 |
Redundancy | 3.7 | 3.7 | 3.5 |
CC(1/2) | 0.989 | 0.577 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 20% PEG5000MME, 0.2mM Ammonium sulfate |