5DNW
Crystal structure of KAI2-like protein from Striga (apo state 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 95 |
Detector technology | IMAGE PLATE |
Collection date | 2013-09-26 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.542 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 75.940, 75.940, 181.470 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.740 - 2.020 |
R-factor | 0.1798 |
Rwork | 0.177 |
R-free | 0.22462 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vxk |
RMSD bond length | 0.009 |
RMSD bond angle | 1.310 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.740 | 2.070 |
High resolution limit [Å] | 2.020 | 2.020 |
Rmerge | 0.370 | |
Number of reflections | 21039 | |
<I/σ(I)> | 36.2 | 6.1 |
Completeness [%] | 99.6 | 96.5 |
Redundancy | 18.7 | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 278 | sodium formate, Tris |