5DJZ
Fc Heterodimer Design 7.8 D399M/Y407A + T366V/K409V
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 193 |
Detector technology | CCD |
Collection date | 2014-07-02 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97931 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.611, 59.629, 149.707 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.810 - 1.900 |
R-factor | 0.23398 |
Rwork | 0.232 |
R-free | 0.27662 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.590 |
Data scaling software | SCALA (3.3.20) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0017) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.814 | 29.814 | 2.000 |
High resolution limit [Å] | 1.900 | 6.010 | 1.900 |
Rmerge | 0.086 | 0.449 | |
Rmeas | 0.130 | ||
Rpim | 0.051 | 0.044 | 0.211 |
Total number of observations | 157002 | 5288 | 20562 |
Number of reflections | 26283 | ||
<I/σ(I)> | 8.8 | 14.4 | 3.1 |
Completeness [%] | 98.3 | 95.4 | 94.7 |
Redundancy | 6 | 5.7 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | 15% PEG 6K + 10mM Magnesium Chloride + 50mM Potassium Chloride |