5DG1

Sugar binding protein - human galectin-2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SEALED TUBE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2015-04-23
Detector	RIGAKU RAXIS
Wavelength(s)	1.5418
Spacegroup name	P 2 21 21
Unit cell lengths	38.500, 106.780, 182.110
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.057 - 3.200
R-factor	0.2997
Rwork	0.297
R-free	0.32080
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1hlc
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.060
High resolution limit [Å]	3.200
Number of reflections	13129
<I/σ(I)>	10.8
Completeness [%]	100.0
Redundancy	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Sodium citrate, Amino Sulfate