Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-G |
| Synchrotron site | APS |
| Beamline | 21-ID-G |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-11-10 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 0.97 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 59.609, 79.313, 87.658 |
| Unit cell angles | 90.00, 94.08, 90.00 |
Refinement procedure
| Resolution | 29.372 - 1.760 |
| R-factor | 0.1938 |
| Rwork | 0.193 |
| R-free | 0.24050 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.802 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.760 |
| Number of reflections | 79247 |
| <I/σ(I)> | 11 |
| Completeness [%] | 98.3 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 15-25% PEG3350 |
