5DDZ
Crystal structure of the RTA-c10-P2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-11-24 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 0.9792 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.626, 67.626, 140.652 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.010 - 1.500 |
R-factor | 0.14767 |
Rwork | 0.146 |
R-free | 0.17520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2aai |
RMSD bond length | 0.009 |
RMSD bond angle | 1.240 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.010 |
High resolution limit [Å] | 1.500 |
Number of reflections | 52756 |
<I/σ(I)> | 26.5 |
Completeness [%] | 99.7 |
Redundancy | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.4 M ammonium dihydrogen phosphate |