5DCN
Crystal structure of LC3 in complex with TECPR2 LIR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2015-05-09 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.99987 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.705, 60.705, 99.946 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.489 - 2.000 |
R-factor | 0.2131 |
Rwork | 0.209 |
R-free | 0.24730 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.648 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.870 |
High resolution limit [Å] | 2.000 |
Number of reflections | 14950 |
<I/σ(I)> | 24.2 |
Completeness [%] | 99.8 |
Redundancy | 19.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.8M Lithium sulphate, 0.01M Magnesium chloride, 0.05M MES monohydrate, pH5.6 |