5DCK
Crystal Structure of FIV Capsid C-Terminal Domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-X |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-09-17 |
| Detector | RIGAKU RAXIS HTC |
| Wavelength(s) | 1.54178 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 64.190, 64.190, 178.560 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.630 - 2.290 |
| R-factor | 0.23777 |
| Rwork | 0.235 |
| R-free | 0.28683 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3dtj |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.515 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER (2.5.6) |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.630 | 2.372 |
| High resolution limit [Å] | 2.290 | 2.290 |
| Rmerge | 0.108 | 0.529 |
| Number of reflections | 10456 | |
| <I/σ(I)> | 17.91 | 2.92 |
| Completeness [%] | 99.7 | 96.96 |
| Redundancy | 16.3 | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.2 | 293 | 0.056M Sodium phosphate monobasic monohydrate, 1.344M Pottasium phosphate dibasic |
