Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.12709 |
Spacegroup name | P 63 |
Unit cell lengths | 90.690, 90.690, 74.713 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.800 - 1.730 |
R-factor | 0.16802 |
Rwork | 0.166 |
R-free | 0.20213 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 2.026 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.800 |
High resolution limit [Å] | 1.730 |
Number of reflections | 36195 |
<I/σ(I)> | 10 |
Completeness [%] | 99.7 |
Redundancy | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.7 | 298 | 4M SODIUM FORMATE, 1% PEG 4000, PH 9.7 |