5D5Z
Structure of Chaetomium thermophilum Skn7 coiled-coil domain, crystal form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 47.004, 61.027, 75.794 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.700 |
R-factor | 0.2131 |
Rwork | 0.209 |
R-free | 0.28530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5d5y |
RMSD bond length | 0.020 |
RMSD bond angle | 1.981 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP (11.0.05) |
Refinement software | REFMAC (2.7.029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.530 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.104 | 0.808 |
Number of reflections | 24701 | |
<I/σ(I)> | 10.5 | 2.2 |
Completeness [%] | 99.9 | 98.3 |
Redundancy | 8.8 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 21 % PEG-6000 |