5D5Y
Structure of Chaetomium thermophilum Skn7 coiled-coil domain, crystal form I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97857 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 24.823, 151.535, 47.745 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.030 |
R-factor | 0.1664 |
Rwork | 0.165 |
R-free | 0.19900 |
Structure solution method | SAD |
RMSD bond length | 0.022 |
RMSD bond angle | 1.853 |
Data reduction software | XDS |
Data scaling software | Aimless (0.1.27) |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.390 | 40.390 | 1.050 |
High resolution limit [Å] | 1.030 | 5.630 | 1.030 |
Rmerge | 0.066 | 0.066 | 1.103 |
Rpim | 0.020 | 0.023 | 0.495 |
Total number of observations | 514459 | 3491 | 9642 |
Number of reflections | 45013 | ||
<I/σ(I)> | 17.1 | 40.1 | 1.5 |
Completeness [%] | 98.7 | 99.8 | 80.8 |
Redundancy | 11.4 | 10.1 | 5.4 |
CC(1/2) | 0.998 | 0.996 | 0.680 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 20 % PEG-6000, 0.1 M HEPES-NaOH pH 7.0 |