5D4R
Crystal Structure of AraR(DBD) in complex with operator ORE1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-03-09 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 134.081, 42.433, 67.232 |
| Unit cell angles | 90.00, 114.82, 90.00 |
Refinement procedure
| Resolution | 36.000 - 2.070 |
| R-factor | 0.1999 |
| Rwork | 0.197 |
| R-free | 0.24710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4h0e |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.226 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 36.000 |
| High resolution limit [Å] | 2.070 |
| Number of reflections | 21116 |
| <I/σ(I)> | 10 |
| Completeness [%] | 99.2 |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 295 | sodium acetate, PEG 8000, Potassium chloride |
