5D2A

Bifunctional dendrimers

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-12-19
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1.0000
Spacegroup name	P 63 2 2
Unit cell lengths	105.107, 105.107, 111.092
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.506 - 2.134
R-factor	0.2091
Rwork	0.205
R-free	0.24600
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4ce8
RMSD bond length	0.010
RMSD bond angle	1.320
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	47.506
High resolution limit [Å]	2.130
Number of reflections	38033
<I/σ(I)>	14.95
Completeness [%]	99.5
Redundancy	10.28

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	292	2M sodium chloride