5D1F

Crystal structure of maize PDRP bound with AMP and Hg2+

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-5A
Synchrotron site	Photon Factory
Beamline	BL-5A
Temperature [K]	100
Detector technology	CCD
Collection date	2013-06-20
Detector	ADSC QUANTUM 315
Wavelength(s)	1
Spacegroup name	P 4 3 2
Unit cell lengths	175.514, 175.514, 175.514
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.680 - 3.400
R-factor	0.22404
Rwork	0.223
R-free	0.24273
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.456
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	3.400
Rmerge	0.092
Number of reflections	13309
<I/σ(I)>	55.5
Completeness [%]	100.0
Redundancy	217.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	277	peg, dioxane