5D0Q
BamACDE complex, outer membrane beta-barrel assembly machinery (BAM) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 197 |
Detector technology | PIXEL |
Collection date | 2015-05-12 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 254.157, 254.157, 179.215 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.943 - 3.500 |
R-factor | 0.3154 |
Rwork | 0.314 |
R-free | 0.33990 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.186 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | SHELXDE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.940 | 3.580 |
High resolution limit [Å] | 3.500 | 3.500 |
Number of reflections | 74050 | |
<I/σ(I)> | 8.2 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 26.9 | 24.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 297 | 0.1 M Tris, pH8.0, 0.1 M MgCl2, 24% PEG500 MME. |