5CZC
The structure of VinK
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-11-07 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.520, 74.810, 84.810 |
| Unit cell angles | 90.00, 91.24, 90.00 |
Refinement procedure
| Resolution | 42.430 - 1.800 |
| R-factor | 0.16795 |
| Rwork | 0.165 |
| R-free | 0.21611 |
| Structure solution method | SAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.827 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.510 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.104 | 0.490 |
| Number of reflections | 52383 | |
| <I/σ(I)> | 7.8 | 2.2 |
| Completeness [%] | 99.3 | 99.3 |
| Redundancy | 3.3 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 299 | 0.1 M calcium acetate, 20% polyethylene glycol 3350 |
