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5CVI

Structure of the manganese regulator SloR

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 4.2.2
Synchrotron siteALS
Beamline4.2.2
Temperature [K]100
Detector technologyCCD
Collection date2013-04-22
DetectorNOIR-1
Wavelength(s)0.9785
Spacegroup nameP 41 21 2
Unit cell lengths60.432, 60.432, 298.780
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution59.230 - 2.804
R-factor0.2025
Rwork0.200
R-free0.25840
Structure solution methodSAD
RMSD bond length0.003
RMSD bond angle0.565
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]59.2302.960
High resolution limit [Å]2.8002.800
Rmerge0.0980.532
Number of reflections25853
<I/σ(I)>255.1
Completeness [%]99.798.9
Redundancy7.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.529312% PEG 3350, 40 mM lithium sulfate, 1 mM zinc chloride

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