5CU3
Crystal structure of CK2alpha bound to CAM4066
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-26 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9173 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 65.280, 66.333, 333.618 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.600 - 1.787 |
R-factor | 0.1845 |
Rwork | 0.183 |
R-free | 0.20180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3war |
RMSD bond length | 0.011 |
RMSD bond angle | 0.970 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.4) |
Phasing software | PHASER |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.600 | 1.793 |
High resolution limit [Å] | 1.787 | 1.787 |
Rmerge | 0.045 | 0.638 |
Rpim | 0.020 | 0.185 |
Total number of observations | 437940 | 108470 |
Number of reflections | 69228 | |
<I/σ(I)> | 20.2 | 2.1 |
Completeness [%] | 100.0 | 99.6 |
Redundancy | 6.3 | 4.9 |
CC(1/2) | 1.000 | 0.927 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 107mM Mes pH 6.5, 29% glycerol ethoxylate, 1 M ammonium acetate |