5CSC
STRUCTURE OF AN OPEN FORM OF CHICKEN HEART CITRATE SYNTHASE AT 2.8 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 43 |
Unit cell lengths | 58.850, 58.850, 259.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.800 |
R-factor | 0.197 |
RMSD bond length | 0.024 |
RMSD bond angle | 3.300 |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.700 * | 2.700 * |
Rmerge | 0.139 * | |
Total number of observations | 53801 * | |
Number of reflections | 15130 * | |
Completeness [%] | 62.4 * | 22 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | citrate | 0.5 (M) | |
3 | 1 | drop | CoA | 10 (mM) | |
4 | 1 | reservoir | sodium citrate | 1.0 (M) |