Experimental procedure
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Temperature [K] | 290 |
Detector technology | FILM |
Detector | FILM |
Spacegroup name | H 3 2 |
Unit cell lengths | 91.600, 91.600, 268.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.193 * |
Rwork | 0.193 |
Structure solution method | MIR |
RMSD bond length | 0.019 |
RMSD bond angle | 19.578 * |
Data reduction software | OSCTST |
Data scaling software | CCP4 ((ROTAVATA)) |
Phasing software | NEWREF ((LYNN TEN EYCK)) |
Refinement software | TNT (1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.096 |
Number of reflections | 17141 |
Completeness [%] | 84.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 7.5 | or batch * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 42 (%sat) | |
2 | 1 | 1 | phosphate | 1.2 (M) |