5CPP
THE STRUCTURAL BASIS FOR SUBSTRATE-INDUCED CHANGES IN REDOX POTENTIAL AND SPIN EQUILIBRIUM IN CYTOCHROME P-450(CAM)
Experimental procedure
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 108.670, 103.900, 36.380 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 * - 2.080 |
| R-factor | 0.19 |
| RMSD bond length | 0.028 |
| RMSD bond angle | 0.040 * |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.080 * |
| Rmerge | 0.061 * |
| Total number of observations | 54729 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | P-450CAM | 1 (mM) | camphor free |
| 2 | 1 | 1 | 250 (mM) | ||
| 3 | 1 | 1 | dithiothreitol | 50 (mM) | |
| 4 | 1 | 2 | ammonium sulfate | 66-70 (%sat) | with 5M KOH |
