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5CE7

Structure of a non-canonical CID of Ctk3

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2011-06-29
DetectorPSI PILATUS 6M
Wavelength(s)0.97964, 0.98012 ,0.97197
Spacegroup nameP 43 21 2
Unit cell lengths51.310, 51.310, 119.050
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution47.120 - 2.000
R-factor0.1917
Rwork0.189
R-free0.24100
Structure solution methodMAD
RMSD bond length0.008
RMSD bond angle1.047
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareSOLVE
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]47.1202.050
High resolution limit [Å]2.0008.9502.000
Rmerge0.0770.0220.456
Rmeas0.0830.0230.488
Total number of observations157934
Number of reflections205242331556
<I/σ(I)>20.8970.434.93
Completeness [%]100.010099.9
Redundancy7.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION4277PEG 6000, citric acid, lithium chloride

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