5CE7
Structure of a non-canonical CID of Ctk3
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-06-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97964, 0.98012 ,0.97197 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 51.310, 51.310, 119.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.120 - 2.000 |
R-factor | 0.1917 |
Rwork | 0.189 |
R-free | 0.24100 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.047 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.120 | 2.050 | |
High resolution limit [Å] | 2.000 | 8.950 | 2.000 |
Rmerge | 0.077 | 0.022 | 0.456 |
Rmeas | 0.083 | 0.023 | 0.488 |
Total number of observations | 157934 | ||
Number of reflections | 20524 | 233 | 1556 |
<I/σ(I)> | 20.89 | 70.43 | 4.93 |
Completeness [%] | 100.0 | 100 | 99.9 |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4 | 277 | PEG 6000, citric acid, lithium chloride |