5C8O
Crystal structure of MoCVNH3 variant (Mo0v)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-01 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.411, 51.075, 43.243 |
Unit cell angles | 90.00, 110.62, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.410 | 2.160 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.073 | 0.179 |
Number of reflections | 9051 | |
<I/σ(I)> | 10.5 | 2.1 |
Completeness [%] | 99.2 | 96.7 |
Redundancy | 2.66 | 1.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 298 | ~8-10 % (w/v) PEG 3350, 0.1 M sodium phosphate-citrate buffer, pH 4.2, 0.2 M NaCl |