5C6G
Structural Insights into the Scc2-Scc4 Cohesin Loader
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.92 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 112.240, 88.810, 116.000 |
Unit cell angles | 90.00, 118.49, 90.00 |
Refinement procedure
Resolution | 98.648 - 2.600 |
R-factor | 0.2297 |
Rwork | 0.227 |
R-free | 0.27430 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.231 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | SHARP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.660 | 2.620 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.040 | 0.591 |
Number of reflections | 63440 | |
<I/σ(I)> | 17.96 | |
Completeness [%] | 96.8 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG 6000, cacodylate. calcium acetate |