5C4R
CobK precorrin-6A reductase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-06-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.13956 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.900, 75.300, 115.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.010 - 3.170 |
R-factor | 0.18194 |
Rwork | 0.179 |
R-free | 0.23595 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.597 |
Data scaling software | Aimless |
Phasing software | SHELX |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.010 | 3.340 |
High resolution limit [Å] | 3.170 | 3.170 |
Rmerge | 0.596 | |
Number of reflections | 16610 | |
<I/σ(I)> | 5.5 | 2.6 |
Completeness [%] | 98.2 | 97 |
Redundancy | 1.8 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 291 | 18% PEG3350, 0.2M NH4Cl |