5C4N

CobK precorrin-6A reductase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-06-28
Detector	DECTRIS PILATUS 2M
Wavelength(s)	0.978
Spacegroup name	P 21 21 21
Unit cell lengths	33.870, 73.140, 103.220
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.170 - 1.630
R-factor	0.17632
Rwork	0.175
R-free	0.20820
RMSD bond length	0.021
RMSD bond angle	2.303
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0049)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.170	1.720
High resolution limit [Å]	1.630	1.630
Number of reflections	32962
<I/σ(I)>	19.4	4.4
Completeness [%]	100.0	100
Redundancy	7.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	291	100