5BXF

Apo FcRn Structure at pH 4.5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 4.2.2
Synchrotron site	ALS
Beamline	4.2.2
Temperature [K]	80
Detector technology	CCD
Collection date	2011-03-21
Detector	ADSC QUANTUM 210
Wavelength(s)	.997
Spacegroup name	P 1 21 1
Unit cell lengths	42.183, 77.583, 140.546
Unit cell angles	90.00, 93.60, 90.00

Refinement procedure

Resolution	46.756 - 2.851
R-factor	0.2415
Rwork	0.237
R-free	0.31380
RMSD bond length	0.010
RMSD bond angle	1.554
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.760
High resolution limit [Å]	2.850
Number of reflections	21222
<I/σ(I)>	12.2
Completeness [%]	99.3
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	.1M sodium citrate pH 4.5, 20% PEG (4000)