5BXF
Apo FcRn Structure at pH 4.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2011-03-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | .997 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.183, 77.583, 140.546 |
Unit cell angles | 90.00, 93.60, 90.00 |
Refinement procedure
Resolution | 46.756 - 2.851 |
R-factor | 0.2415 |
Rwork | 0.237 |
R-free | 0.31380 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.554 |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.760 |
High resolution limit [Å] | 2.850 |
Number of reflections | 21222 |
<I/σ(I)> | 12.2 |
Completeness [%] | 99.3 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | .1M sodium citrate pH 4.5, 20% PEG (4000) |