5BXC
Crystal structure of GTA + UDP + DI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2007-10-25 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 52.650, 148.860, 80.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.330 - 1.400 |
R-factor | 0.18124 |
Rwork | 0.180 |
R-free | 0.20061 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lz0 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.507 |
Data reduction software | CrystalClear (1.3.6 SP2 r1) |
Data scaling software | d*TREK (9.4SSI) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.330 | |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.033 | 0.307 |
Number of reflections | 59210 | |
<I/σ(I)> | 20.4 | 3.1 |
Completeness [%] | 95.1 | 81.4 |
Redundancy | 4.07 | 2.54 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 1 % PEG 4000, 4.5-5 % 2-methyl-2,4-pentanediol (MPD), 100 mM ammonium sulfate, 70 mM sodium chloride, 50 mM N-[2-acetamido]-2-iminodiacetic acid (ADA), 30 mM sodium acetate, 5-8 mM cobalt chloride, pH 7.5 |