Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-05-06 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.91790 |
| Spacegroup name | P 1 |
| Unit cell lengths | 57.002, 73.812, 77.633 |
| Unit cell angles | 83.21, 66.41, 70.66 |
Refinement procedure
| Resolution | 15.000 - 2.500 |
| R-factor | 0.2116 |
| Rwork | 0.209 |
| R-free | 0.25970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3c9i |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.787 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.000 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 37023 | |
| <I/σ(I)> | 9.04 | 2.327 |
| Completeness [%] | 98.1 | 95 |
| Redundancy | 1.9 | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9 | 289 | 40% PEG 4000, 0.1M potassium chloride, 0.1M TAPS buffer, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 289K |
